国际口腔医学杂志 ›› 2014, Vol. 41 ›› Issue (3): 272-276.doi: 10.7518/gjkq.2014.03.006

• 论著 • 上一篇    下一篇

酸性环境下饰面瓷的摩擦磨损行为研究

张倩倩1 丘小丽2 高姗姗1 于海洋1   

  1. 1.口腔疾病研究国家重点实验室 华西口腔医院(四川大学) 成都 610041; 2.南宁市第二人民医院口腔科 南宁 530031
  • 收稿日期:2013-10-28 修回日期:2014-03-03 出版日期:2014-05-01 发布日期:2014-05-01
  • 通讯作者: 于海洋,教授,博士,Email:yhyang6812@scu.edu.cn
  • 作者简介:张倩倩,硕士,Email:zhangqianqian8729@163.com
  • 基金资助:

    国家自然科学基金(81100777,81170996);高等学校博士学科点专项科研基金(20110181120076)

Friction and wear behavior of two kinds of veneering porcelains in an acidic environment

Zhang Qianqian1, Qiu Xiaoli2, Gao Shanshan1, Yu Haiyang1   

  1. 1. State Key Laboratory of Oral Diseases, West China Hospital of Stomatology, Sichuan University, Chengdu 610041, China; 2. Dept. of Stomatology, Nanning Second People’s Hospital, Nanning 530031, China
  • Received:2013-10-28 Revised:2014-03-03 Online:2014-05-01 Published:2014-05-01

摘要:

目的 研究在酸性饮料环境中2种饰面瓷Vita master和Ceramco 3的摩擦磨损行为。方法 采用努氏显微硬度仪测其表面硬度;在可口可乐环境下通过Plint微动磨损实验机评价饰面瓷的摩擦磨损性能并对磨斑进行三维重建,用表面轮廓仪测量磨痕深度,计算磨损体积。用扫描电子显微镜和激光共聚焦扫描显微镜观察饰面瓷的微观结构和表面磨损形貌特征。对Vita master和Ceramco 3的努氏硬度、磨斑体积和平均磨损深度进行t检验。结果 2种饰面瓷的微观结构不同,酸蚀后Vita master的晶体呈现融合现象,Ceramco 3的晶体呈现脆性脱落。Vita master的硬度低于Ceramco 3的硬度,但Vita master的磨损深度、磨损体积和稳定摩擦系数也低于Ceramco 3。Vita master的三维重建磨斑为带有犁沟的不规则四边形;磨损形貌主要为粗大而深且密集均匀分布的犁沟。Ceramco 3的三维重建磨斑为规则的椭圆形;磨损形貌主要为剥层和磨屑。结论 2种饰面瓷的硬度和酸性介质下的摩擦磨损行为没有直接关系;在酸性饮料环境下,Vita master和Ceramco 3的摩擦磨损行为存在较大差异,Vita master的磨损机制以磨粒磨损为主;Ceramco 3的磨损机制主要为裂纹的萌生和扩展。

关键词: 饰面瓷, 摩擦磨损, 磨损机制, 酸性环境

Abstract:

Objective This study examines the friction and wear behavior of Vita master and Ceramco 3 in an acidic environment. Methods Surface microhardness was measured using a microhardness tester. Wear tests were performed on a ball-on-disc plint fretting wear under Coca Cola. The wear depth was measured by a surface profiler, and wear volume was calculated. Wear scars were reconstructed in three dimensions. The microstructure and wear surface morphologies were investigated using a scanning electron microscope and a laser confocal scanning microscope. Finally, the Knoop hardness and wear amount of porcelains were evaluated via t test. Results The microstructures of two kinds of materials differed. The interfaces of Vita master between the crystal and the matrix were not angled for crystal etching. As for Ceramco 3, the leucite crystals were completely removed from the matrix after etching. The hardness, wear volume, wear depth, and friction coefficient of Vita master were lower than those of Ceramco 3. The wear surface of Vita master was trapezoidal, with a scratch and wear morphology characterized by plough. By contrast, the wear surface of Ceramco 3 was a smooth oval, and its wear morphology was characterized by delamination and abrasive grains. Conclusion No significant correlation was detected between hardness value and wear volume in an acidic environment. Significant differences were observed between Vita master and Ceramco 3 in terms of friction and wear behavior in the Coca Cola test. The wear mechanism of Vita master is abrasive, whereas that of Ceramco 3 is the initiation and propagation of cracks.

Key words: veneering porcelain, friction and wear, wear mechanism, acid environment

中图分类号: 

  • R 783
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